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TOB NEW ENERGYitem no.:
TOB-AKF-CH6order(moq):
1 setPayment:
L/C,T/Tproduct origin:
Chinashipping port:
XIAMEN
SPECIFICATIONS（Contact us for more information and demo videos）
TOB-AKF-CH6 Karl Fischer moisture measurement equipment with moisture measurement module and feeding sample heating module function together, it’s completely in accordance with the needs of lithium industry users, novel design, easy to use and maintenance, can fully cover the lithium battery industry from anode and cathode materials, electrode, separator and electrolyte; Moisture ranges from 1ppm to 100% of use requirements.
Advantage:
1. The equipment occupies less space and is more convenient to operate. For the lithium battery industry, especially for customers equipped with glove boxes, the all-in-one machine is more suitable.
2. Automatic lifting puncture, effectively save manpower, improve analysis efficiency.
3. Optimized some functions of the software to make the test more stable and convenient, and added functions such as user management and permissions to facilitate the management of the test process.
Feature
● Karl furnace and moisture meter integrated pioneered design in China, reasonable layout, less space occupation.
● Color touch screen, full digital keyboard, one button start, easy to operate, without professionals can easily work.
● HOGON intelligent detection technology: automatic balance, automatic detection, adapt to the environment drift automatically adjust detection accuracy.
● New electrolytic control ability, adapt to all kinds of electrolyte, high detection limit, moisture determination accuracy up to 0.01ug.
● With carrier gas flow electronic display, moisture content curve display and other functions, intuitive interface.
● Sample evaporator with constant temperature, Temperature programmed and other high precision temperature control mode, and with intelligent over temperature protection function.
● Automatic lifting puncture function plus rotary cover double injection mode, can be flexibly selected according to different use environment.
● Can edit, store, call a variety of different analysis method parameters, easy to adapt to different sample detection.
● Equipped with a variety of determination methods, and adapt to the gas, liquid, fixed samples and high and low water content of a variety of detection needs.
● Intelligent state monitoring, hardware intelligent protection, abnormal termination, timing stop and other capabilities, effectively extend the service life of the product.
|
Measure Method |
Karl FischerCoulomb method (Coulometry) |
|
Measure Range |
H2O：3ug-199mg/0.01ug(H2O mass） Measurement resolution: 0.01ug(H2O mass) |
|
Measure repeatability |
≧99.7%（1000μgH2O） |
|
Applicable sample type |
Liquid,solid,gas |
|
Sample feeding method |
Direct feeding, puncture feeding, change cover and purge feeding |
|
Temperature control range |
RT~285℃ /0.1℃；3 level Temperature programmed |
|
Heating rate |
15℃/min（under 200℃） |
|
Measure duration |
Average 50 seconds to 10 minutes (methods vary) |
|
Input gas source |
External dry air/nitrogen (99.99%) |
|
Carrier gas pressure |
Input limit: 0.6mpa, output: 0-0.4mpa |
|
Flow range |
0~100mL/min |
|
Flow accuracy |
1ml/min |
|
Sample bottle specification |
10ml |
|
Data output |
RS232/USB,USB pin micro printer |
|
Instrument power |
300W；220V/50Hz |
|
Size, weight |
L500*W250*H360（mm）Weight：11.5（kg） |
Application to Cathode Electrode, Electrolyte and Separator
Karl Fischer Coulometry for Cathode Electrode Moisture Measure
| Abstract |
Electrode sheet is an important part of finished lithium battery,
which is generally divided into cathode and anode electrode sheet. In this
experiment, use TOB-AKF-CH6 all-in-one machine to measure the moisture
content of cathode electrode sample. Experimental conditions: ambient temperature 25℃; Ambient humidity≤30% |
| Sample | Cathode electrode |
| Measure method |
1. Turn on the TOB-AKF-CH6 moisture tester and add an appropriate
amount of Karl Fischer reagent to the titration tank to ensure that the
reagent is between the maximum and minimum scale. 2. Before opening the nitrogen cylinder, set and adjust the air volume and temperature. 3. Wait for blank electrolysis balance test of the instrument. 4. For sample testing, take appropriate amount of sample into the sample bottle, place it on the heating tank, connect the heating tracing tube, click start measurement, then sample, input relevant parameters, and wait for the measurement results |
Results
|
No. |
Sample qty/g |
Water content/ug |
Measure duration/nin |
Result/ppm |
|
1 |
0.6718 |
203.9 |
5:00 |
303.5 |
|
2 |
0.6383 |
182.1 |
5:00 |
285.3 |
|
3 |
0.6569 |
187.6 |
5:00 |
285.6 |
Karl Fischer Coulometry For Electrolyte Moisture Measure
|
Abstract |
Lithium battery electrolyte is the carrier of ion transport in the battery, which is generally composed of lithium salts and organic solvents. TOB-AKF-CH6 was used to measure the water content in the electrolyte sample. Experimental conditions: ambient temperature 25℃; Ambient humidity 35% |
|
Sample |
Electrolyte |
|
Measure method |
1. Turn on the TOB-AKF-CH6 moisture tester and add an appropriate amount of Karl Fischer reagent to the titration tank to ensure that the reagent is between the maximum and minimum scale. 2. Close the nitrogen cylinder 3. Wait for blank electrolysis balance test of the instrument. 4. For sample testing, take appropriate amount of sample into the sample bottle, place it on the heating tank, connect the heating tracing tube, click start measurement, then sample, input relevant parameters, and wait for the measurement results |
Results
|
No. |
Sample qty/g |
Water content/ug |
Measure duration/nin |
Result/ppm |
|
1 |
0.62 |
5.1 |
1:06 |
8.2 |
|
2 |
0.61 |
5.4 |
1:18 |
8.9 |
|
3 |
0.65 |
5.0 |
1:25 |
7.7 |
Karl Fischer Coulometry For Separator Moisture Measure
|
Abstract |
In the structure of lithium battery, separator is one of the key inner components. AKF-CH6 was used to measure moisture content in separator samples.
Experimental conditions: ambient temperature 25℃; Ambient humidity 35% |
|
Sample |
Separator |
|
Measure method |
1. Turn on the TOB-AKF-CH6 moisture tester and add an appropriate amount of Karl Fischer reagent to the titration tank to ensure that the reagent is between the maximum and minimum scale. 2. Turn on the nitrogen cylinder,set gas flow,temperature 3. Wait for blank electrolysis balance test of the instrument. 4. For sample testing, take appropriate amount of sample into the sample bottle, place it on the heating tank, connect the heating tracing tube, click start measurement, then sample, input relevant parameters, and wait for the measurement results |
Results
|
No. |
Sample qty/g |
Water content/ug |
Measure duration/nin |
Result/ppm |
|
1 |
0.1505 |
23.4 |
4:11 |
155.5 |
|
2 |
0.1532 |
27.8 |
4:14 |
181.4 |
|
3 |
0.1887 |
39.3 |
4:15 |
208.3 |
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